C₂₃H₂₈Cl₂N₂O₅

Base Information

Chemical Name:C₂₃H₂₈Cl₂N₂O₅
CAS No.:1006584-02-6
Molecular Formula:C₂₃H₂₈Cl₂N₂O₅
Molecular Weight:483.392
Hs Code.:

C<sub>23</sub>H<sub>28</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₃H₂₈Cl₂N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₈Cl₂N₂O₅

Chemical Property:

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Technology Process of C₂₃H₂₈Cl₂N₂O₅

There total 4 articles about C₂₃H₂₈Cl₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942998-90-5
ethyl 4-[(2-amino)ethoxy]-3,5-dichlorobenzoate

: 1006584-02-6
C₂₃H₂₈Cl₂N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h / 20 °C

2: lithium hydroxide / tetrahydrofuran / 3 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 16 h

With lithium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z

Reference yield:

: 17302-82-8
ethyl 3,5-dichloro-4-hydroxybenzoate

: 1006584-02-6
C₂₃H₂₈Cl₂N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 120 °C

2: hydrazine hydrate / ethanol / 3 h / 100 °C

3: dichloromethane / 2 h / 20 °C

4: lithium hydroxide / tetrahydrofuran / 3 h / 20 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 16 h

With lithium hydroxide; potassium carbonate; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z

Reference yield:

: 942998-89-2
ethyl 3,5-dichloro-4-[2-(1,3-dioxo-1,3-dihydroisoindol-2-yl)ethoxy]benzoate

: 1006584-02-6
C₂₃H₂₈Cl₂N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / ethanol / 3 h / 100 °C

2: dichloromethane / 2 h / 20 °C

3: lithium hydroxide / tetrahydrofuran / 3 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 16 h

With lithium hydroxide; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z