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C55H83O6Si3N

Base Information
  • Chemical Name:C55H83O6Si3N
  • CAS No.:936824-95-2
  • Molecular Formula:C55H83NO6Si3
  • Molecular Weight:938.524
  • Hs Code.:
C<sub>55</sub>H<sub>83</sub>O<sub>6</sub>Si<sub>3</sub>N

Synonyms:C55H83O6Si3N

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Chemical Property of C55H83O6Si3N
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Technology Process of C55H83O6Si3N

There total 7 articles about C55H83O6Si3N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/ol0702270
Guidance literature:
Multi-step reaction with 6 steps
1.1: Cp2ZrCl2 / hexane; 1,2-dichloro-ethane / 0.83 h / 0 - 20 °C
1.2: 1,2-dichloro-ethane; hexane / 72 h / 20 °C
1.3: 58 percent / iodine / 1,2-dichloro-ethane; hexane; tetrahydrofuran / -30 - 0 °C
2.1: 89 percent / pyridine / CH2Cl2 / 3 h / 0 °C
3.1: 79 percent / Pd(PPh3)4 / dimethylformamide / 4 h / 55 °C
4.1: 48 percent / anhydrous ZnCl2 / nitromethane / 1 h / sonication
5.1: 89 percent / imidazole; DMAP / CH2Cl2 / 1.5 h / 20 °C
6.1: 60 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic acid chloride; DIEA / CH2Cl2 / 18 h / 20 °C
With pyridine; 1H-imidazole; dmap; zirconocene dichloride; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0); In nitromethane; hexane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 3.1: Stille coupling;
DOI:10.1021/ol0702270
Guidance literature:
Multi-step reaction with 5 steps
1: 89 percent / pyridine / CH2Cl2 / 3 h / 0 °C
2: 79 percent / Pd(PPh3)4 / dimethylformamide / 4 h / 55 °C
3: 48 percent / anhydrous ZnCl2 / nitromethane / 1 h / sonication
4: 89 percent / imidazole; DMAP / CH2Cl2 / 1.5 h / 20 °C
5: 60 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic acid chloride; DIEA / CH2Cl2 / 18 h / 20 °C
With pyridine; 1H-imidazole; dmap; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0); In nitromethane; dichloromethane; N,N-dimethyl-formamide; 2: Stille coupling;
DOI:10.1021/ol0702270
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