2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

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Chemical Name:2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester
CAS No.:249922-65-4
Molecular Formula:C₄₁H₅₁N₃O₃
Molecular Weight:633.874
Hs Code.:

Synonyms:2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

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Chemical Property of 2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

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Technology Process of 2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

There total 4 articles about 2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 249922-62-1
(S)-2,5-Bis(N,N-dibenzylamino)-1-pentanol

: 249922-65-4
2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

Guidance literature:: (S)-2,5-Bis(N,N-dibenzylamino)-1-pentanol; With sodium hydride; In tetrahydrofuran; for 1h; Heating;

2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride; In tetrahydrofuran; for 6h; Heating;
DOI:10.1055/s-1999-3575

Reference yield:

: 100-39-0
benzyl bromide

: 249922-65-4
2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃; NaOH / aq. methanol / 1 h / Heating

2.1: LiAlH₄ / tetrahydrofuran / Heating

3.1: NaH / tetrahydrofuran / 1 h / Heating

3.2: 83 percent / tetrahydrofuran / 6 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; 1.1: Alkylation / 2.1: Reduction / 3.1: Metallation / 3.2: Acylation;
DOI:10.1055/s-1999-3575

Reference yield:

: 3184-13-2,36630-89-4
L-ornithine hydrochloride

: 249922-65-4
2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (S)-2,5-bis-dibenzylamino-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃; NaOH / aq. methanol / 1 h / Heating

2.1: LiAlH₄ / tetrahydrofuran / Heating

3.1: NaH / tetrahydrofuran / 1 h / Heating

3.2: 83 percent / tetrahydrofuran / 6 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; 1.1: Alkylation / 2.1: Reduction / 3.1: Metallation / 3.2: Acylation;
DOI:10.1055/s-1999-3575