{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

Base Information

Chemical Name:{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane
CAS No.:1260073-02-6
Molecular Formula:C₂₆H₃₃BrOSi
Molecular Weight:469.537
Hs Code.:

Synonyms:{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

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Chemical Property of {[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

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Technology Process of {[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

There total 1 articles about {[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 852211-47-3
1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-3-yn-1-one

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1260073-02-6
{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

Guidance literature:: 1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-3-yn-1-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.333333h;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 12h;
DOI:10.1039/c1ob06693e

Reference yield:

: 1260073-02-6
{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

: C₂₀H₁₈BrFO

Guidance literature:: With Selectfluor; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1002/adsc.201000411

Reference yield:

: 1260073-02-6
{[1-(4-bromophenyl)-4-(4-tert-butylphenyl)but-1-en-3-yn-1-yl]oxy}(tert-butyl)dimethylsilane

: 1310738-73-8
2-(4-bromophenyl)-5-(4-tert-butylphenyl)-3-fluoro-4-iodofuran

Guidance literature:: Multi-step reaction with 2 steps

1: Selectfluor / acetonitrile / 1 h / 22 °C

2: N-iodo-succinimide; gold(I) chloride; zinc dibromide / dichloromethane / 0.17 h / 20 °C

With N-iodo-succinimide; Selectfluor; gold(I) chloride; zinc dibromide; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201100344