2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Base Information

Chemical Name:2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide
CAS No.:116686-64-7
Molecular Formula:C₁₃H₁₁F₂NO₃S₂
Molecular Weight:331.364
Hs Code.:

Synonyms:2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Suppliers and Price of 2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

There total 8 articles about 2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140-89-6
potassium ethyl xanthogenate

: 116687-66-2
4'-amino-2'-(2,4-difluorophenoxy)methanesulfonanilide

: 116686-64-7
2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Guidance literature:: With hydrogenchloride; potassium hydroxide; sodium borohydrid; sodium nitrite; In methanol; water; ethyl acetate;

Reference yield:

: 367-27-1
2,4-difluorophenol

: 116686-64-7
2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / potassium carbonate / xylene / 5.5 h / Heating

2: iron, ammonium chloride, H₂O / ethanol / 0.5 h / Heating

3: pyridine / 0 °C

4: 81 percent / 71percent aq. nitric acid / 2 h / Ambient temperature

5: ammonium chloride, iron, H₂O / ethanol / 0.5 h / Heating

6: 1.) sodium nitrite, aq. HCl, 2.) potassium ethyl xanthate, 3.) sodium borohydride, potassium hydroxide

With pyridine; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; ammonium chloride; water; nitric acid; potassium ethyl xanthogenate; iron; potassium carbonate; sodium nitrite; In ethanol; xylene;
DOI:10.1248/cpb.40.2399

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 116686-64-7
2'-(2,4-difluorophenoxy)-4'-mercaptomethanesulfonanilide

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / potassium carbonate / xylene / 5.5 h / Heating

2: iron, ammonium chloride, H₂O / ethanol / 0.5 h / Heating

3: pyridine / 0 °C

4: 81 percent / 71percent aq. nitric acid / 2 h / Ambient temperature

5: ammonium chloride, iron, H₂O / ethanol / 0.5 h / Heating

6: 1.) sodium nitrite, aq. HCl, 2.) potassium ethyl xanthate, 3.) sodium borohydride, potassium hydroxide

With pyridine; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; ammonium chloride; water; nitric acid; potassium ethyl xanthogenate; iron; potassium carbonate; sodium nitrite; In ethanol; xylene;
DOI:10.1248/cpb.40.2399