methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

Base Information

Chemical Name:methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate
CAS No.:1462366-85-3
Molecular Formula:C₁₆H₂₄N₂O₃S
Molecular Weight:324.444
Hs Code.:

Synonyms:methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

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Chemical Property of methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

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Technology Process of methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

There total 3 articles about methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1462366-84-2
methyl (S)-2-{[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

: 74-88-4
methyl iodide

: 1462366-85-3
methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc46193a

Reference yield:

: 2491-18-1
(S)-methyl 2-amino-4-(methylthio)butanoate hydrochloride

: 1462366-85-3
methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / 1,2-dimethoxyethane / 0.17 h / Inert atmosphere

1.2: 20 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3cc46193a

Reference yield:

: 52209-63-9
N-methyl-N-(2-methylphenyl)carbamoyl chloride

: 1462366-85-3
methyl (S)-2-{methyl[methyl(2-methylphenyl)carbamoyl]amino}-4-(methylsulfanyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / 1,2-dimethoxyethane / 0.17 h / Inert atmosphere

1.2: 20 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3cc46193a