N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Base Information

Chemical Name:N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide
CAS No.:85838-43-3
Molecular Formula:C₃₂H₅₁N₅O₈S
Molecular Weight:665.852
Hs Code.:

N-<N-acetyl-S-(2-<6-(benzyloxycarbonylamino)hexylamino>-2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Synonyms:N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

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Chemical Property of N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Chemical Property:

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Technology Process of N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

There total 8 articles about N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 85838-43-3
N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / 1.) 12 M HCl; 2.) HCl / 1.) methanol, 18 h; 2.) dichloromethane, 0 deg C

2: 1.) p-nitrophenol, dicyclohexylcarbodiimide / 1.) DMF, 3 h, r.t.; 2.) 2 h

3: 93 percent / sodium hydroxide / ethanol; H₂O / 4 h / Ambient temperature

4: 1.) p-nitrophenol, dicyclohexylcarbodiimide; 2.) triethylamine / 1.) DMF, 3 h, r.t.; 2.) DMF, r.t., overnight

With hydrogenchloride; sodium hydroxide; 4-nitro-phenol; triethylamine; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1016/0008-6215(83)88217-2

Reference yield:

: 1195-16-0,768351-04-8,17896-21-8
N-acetyl-DL-homocysteinethiolactone

: 85838-43-3
N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / triethylamine / CHCl₃ / 4 h / Ambient temperature

2: 66 percent / lead(II) acetate dihydrate / ethanol / Ambient temperature

3: 1.) p-nitrophenol, dicyclohexylcarbodiimide / 1.) DMF, 3 h, r.t.; 2.) 2 h

4: 93 percent / sodium hydroxide / ethanol; H₂O / 4 h / Ambient temperature

5: 1.) p-nitrophenol, dicyclohexylcarbodiimide; 2.) triethylamine / 1.) DMF, 3 h, r.t.; 2.) DMF, r.t., overnight

With sodium hydroxide; 4-nitro-phenol; lead acetate; triethylamine; dicyclohexyl-carbodiimide; In ethanol; chloroform; water;
DOI:10.1016/0008-6215(83)88217-2

Reference yield:

: 78618-06-1
monobenzyloxycarbonyl hexamethylenediamine hydrochloride

: 85838-43-3
N--2-oxoethyl)-DL-homocysteinyl>-N-(5-ethoxycarbonylpentyl)glycinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) p-nitrophenol, dicyclohexylcarbodiimide / 1.) DMF, 3 h, r.t.; 2.) 2 h

2: 93 percent / sodium hydroxide / ethanol; H₂O / 4 h / Ambient temperature

3: 1.) p-nitrophenol, dicyclohexylcarbodiimide; 2.) triethylamine / 1.) DMF, 3 h, r.t.; 2.) DMF, r.t., overnight

With sodium hydroxide; 4-nitro-phenol; triethylamine; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1016/0008-6215(83)88217-2