4-Methyl-2-(methylthio)-3-p-tolyl-thiazoliumiodide

Base Information

• Chemical Name: 4-Methyl-2-(methylthio)-3-p-tolyl-thiazoliumiodide
• CAS No.: 33167-55-4
• Molecular Formula: C12H14 N S2 . I
• Molecular Weight: 363.286
• Hs Code.: 2934100090
• Mol file: 33167-55-4.mol

Synonyms:Thiazolium,4-methyl-2-(methylthio)-3-p-tolyl-, iodide (8CI)

Chemical Property of 4-Methyl-2-(methylthio)-3-p-tolyl-thiazoliumiodide

Chemical Property:

• PSA: 57.42000
• LogP: 0.36750

Purity/Quality:

4-METHYL-2-(METHYLTHIO)-3-P-TOLYL-THIAZOLIUMIODIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methyl-2-(methylthio)-3-p-tolyl-thiazoliumiodide

There total 1 articles about 4-Methyl-2-(methylthio)-3-p-tolyl-thiazoliumiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-methyl-3-(4-methylphenyl)-1,3-thiazole-2(3H)-thione (51655-96-0) + methyl iodide (74-88-4) → 4-methyl-3-(4-methylphenyl)-2-(methylthio)-1,3-thiazol-3-ium iodide (33167-55-4)

Guidance literature:

In acetone; at 20 ℃; for 24h;

DOI:10.1080/00397910701575400

Reference yield: 96.0%

3-Methyl-2-thioxo-thiazolidin-4-on (4807-55-0) + 4-methyl-3-(4-methylphenyl)-2-(methylthio)-1,3-thiazol-3-ium iodide (33167-55-4) → (5E)-3-methyl-5-(4-methyl-3-p-tolylthiazol-2(3H)-ylidene)-2-thioxothiazolidin-4-one

Guidance literature:

With triethylamine; at 50 ℃; for 0.166667h; microwave irradiation;

DOI:10.1080/00397910701575400

Reference yield: 75.0%

3-[6-(4-oxo-2-thioxothiazolidin-3-yl)hexyl]-2-thioxothiazolidin-4-one (21494-66-6) + 4-methyl-3-(4-methylphenyl)-2-(methylthio)-1,3-thiazol-3-ium iodide (33167-55-4) → (5E,5′E)-3,3′-hexane-1,6-diylbis[5-(3-(4-methylphenyl)-4-methyl-1,3-thiazol-2(3H)-ylidene)-2-thioxo-1,3-thiazolidin-4-one]

Guidance literature:

With triethylamine; In dichloromethane; for 3h; Reflux;

DOI:10.1016/j.molstruc.2019.03.077

upstream raw materials:

4-methyl-3-(4-methylphenyl)-1,3-thiazole-2(3H)-thione

methyl iodide

Downstream raw materials:

bis-(4-methyl-3-p-tolyl-3H-thiazol-2-ylidene)-hydrazine

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