tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

Base Information

Chemical Name:tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate
CAS No.:1373693-81-2
Molecular Formula:C₂₉H₄₁NO₅
Molecular Weight:483.648
Hs Code.:

Synonyms:tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

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Chemical Property of tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

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Technology Process of tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

There total 1 articles about tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1373693-80-1
C₂₄H₃₃NO₃

: 1373693-81-2
tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

: 1373693-93-6
tert-butyl (1R)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

Guidance literature:: With dmap; In acetonitrile; at 20 ℃;
DOI:10.1055/s-0031-1290352

Reference yield: 90.0%

: 1373693-81-2
tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

: 1373693-82-3
(S)-5-methyl-3-pentylisobenzofuran-1-(3H)-one

: 64715-80-6
(S)-1-benzyl-2-methoxyethylamine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 100 ℃;
DOI:10.1055/s-0031-1290352

Reference yield:

: 1373693-81-2
tert-butyl (1S)-1-(2-{[(2S)-1-methoxy-3-phenylpropan-2-yl]carbamoyl}-5-methylphenyl)hexyl carbonate

: 1373693-77-6
(S)-N-(1-methoxy-3-phenylpropan-2-yl)-4-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 100 °C

2: thionyl chloride; triethylamine / dichloromethane / 20 °C

With hydrogenchloride; thionyl chloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1055/s-0031-1290352