6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

Base Information

Chemical Name:6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide
CAS No.:935265-54-6
Molecular Formula:C₂₈H₃₉N₃O₃Si
Molecular Weight:493.721
Hs Code.:

Synonyms:6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

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Chemical Property of 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

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Technology Process of 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

There total 1 articles about 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 808134-96-5
1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane

: 70593-61-2
6-chloropyridine-2-carboxamide

: 935265-54-6
6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

Guidance literature:: 1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane; With tert.-butyl lithium;

With tributyltin chloride;

6-chloropyridine-2-carboxamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 24h; Further stages.; Heating;
DOI:10.1021/jm0611509

Reference yield: 77.0%

: 935265-54-6
6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

: 935265-04-6
C₂₂H₂₅N₃O₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jm0611509

Reference yield:

: 935265-54-6
6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinamide

: C₂₂H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Bu₄NF / tetrahydrofuran / 2 h / 20 °C

2: 26 mg / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

With tetrabutyl ammonium fluoride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0611509