2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Base Information

Chemical Name:2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol
CAS No.:166194-06-5
Molecular Formula:C₅₂H₆₉NO₆SSi₂
Molecular Weight:892.36
Hs Code.:

2-<N-(tolylsulfonyl)-N-<4-<(tert-butyldiphenylsilyl)oxy>butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Synonyms:2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Suppliers and Price of 2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

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Chemical Property of 2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

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Technology Process of 2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

There total 5 articles about 2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 166194-06-5
2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / TsOH / CH₂Cl₂ / 2 h / 0 - 20 °C

2: 1.) KH, 2.) 18-crown-6 / 1.) THF, 2.) THF, a) RT, overnight, b) 50 deg C, 6 h

With 18-crown-6 ether; potassium hydride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1021/jm00014a023

Reference yield:

: 130372-07-5
4-(tret-butyldiphenylsilyloxy)butan-1-ol

: 166194-06-5
2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / triphenoxymethylphosphonium iodide / CH₂Cl₂ / -68 - 20 °C

2: 1.) KH, 2.) 18-crown-6 / 1.) THF, 2.) THF, a) RT, overnight, b) 50 deg C, 6 h

With 18-crown-6 ether; methyltriphenoxyphosphonium iodide; potassium hydride; In dichloromethane;
DOI:10.1021/jm00014a023

Reference yield:

: 166193-85-7
2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxazolidinone

: 166194-06-5
2-butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1-(tetrahydropyranyl)-1,4-butanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH, 18-crown-6 / 1.) THF, RT, 30 min, 2.) THF, RT, overnight

2: 82 percent / TsOH / CH₂Cl₂ / 2 h / 0 - 20 °C

3: 1.) KH, 2.) 18-crown-6 / 1.) THF, 2.) THF, a) RT, overnight, b) 50 deg C, 6 h

With 18-crown-6 ether; potassium hydride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1021/jm00014a023