N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Base Information

Chemical Name:N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide
CAS No.:1382468-79-2
Molecular Formula:C₄₄H₃₁NO₉S₂
Molecular Weight:781.863
Hs Code.:

Synonyms:N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

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Chemical Property of N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

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Technology Process of N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

There total 4 articles about N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1382468-82-7
N-cyclohexyl-1,7-bis(p-tolylthio)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

: 1382468-79-2
N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1039/c2cc31087b

Reference yield:

: 1382468-81-6
N,N'-dicyclohexyl-1,7-bis(p-tolylthio)perylene-3,4:9,10-tetracarboxylic acid diimide

: 1382468-79-2
N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium hydroxide / isopropyl alcohol / 3 h / Reflux; Inert atmosphere

2: pyridine; zinc(II) acetate dihydrate / 72 h / 80 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

With pyridine; water; zinc(II) acetate dihydrate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In dichloromethane; isopropyl alcohol;
DOI:10.1039/c2cc31087b

Reference yield:

: 106-45-6
para-thiocresol

: 1382468-79-2
N-cyclohexyl-1,7-bis(p-tolylsulfonyl)perylene-3,4-dicarboxyanhydride-9,10-dicarboximide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammomium bromide; potassium carbonate / 5,5-dimethyl-1,3-cyclohexadiene; water / 2 h / Inert atmosphere; Reflux

2: water; potassium hydroxide / isopropyl alcohol / 3 h / Reflux; Inert atmosphere

3: pyridine; zinc(II) acetate dihydrate / 72 h / 80 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

With pyridine; tetrabutylammomium bromide; water; zinc(II) acetate dihydrate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; isopropyl alcohol;
DOI:10.1039/c2cc31087b