N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

Base Information

• Chemical Name: N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride
• CAS No.: 191997-95-2
• Molecular Formula: C₃₆H₂₈Br₂N₂O₄
• Molecular Weight: 712.437
• Mol file: 191997-95-2.mol

Synonyms:N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

Chemical Property of N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride

There total 13 articles about N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

cyclohexylamine (108-91-8,157973-60-9) + 1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride (118129-60-5) → N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride (191997-95-2)

Guidance literature:

With acetic acid; In 1-methyl-pyrrolidin-2-one; at 85 ℃; for 6h;

DOI:10.1002/anie.200461324

Reference yield: 67.5%

cyclohexylamine (108-91-8,157973-60-9) + perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride (191997-95-2)

Guidance literature:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With sulfuric acid; at 55 ℃; for 24h; Inert atmosphere;

With iodine; at 55 ℃; for 5h; Inert atmosphere;

cyclohexylamine; Further stages;

DOI:10.1002/asia.201700120

Reference yield: 60.0%

N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide (41572-86-5) → N,N'-dicyclohexyl-1,7-dibromoperylene-3,4:9,10-tetracarboxylic dianhydride (191997-95-2)

Guidance literature:

With bromine; In dichloromethane; for 168h; Reflux;

DOI:10.1002/jhet.2883

upstream raw materials:

cyclohexylamine

1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide

Downstream raw materials:

2,9-Dicyclohexyl-5,12-di-pentadec-1-ynyl-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

(N,N'-dicyclohexyl-1-bromo-7-dodecyloxy)perylene-3,4:9,10-tetracarboxydiimide

C₆₄H₇₀N₂O₆

N,N'-dicyclohexyl-1,7-di(3-methoxyphenoxy)perylene-3,4:9,10-tetracarboxylic acid bisimide