Technology Process of C15H20O5
There total 1 articles about C15H20O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
water; tert-butyl alcohol;
at 0 ℃;
DOI:10.3987/COM-09-S(S)93
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran; diethyl ether / -78 °C
2.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0 °C
2.2: 18 h / 30 °C
3.1: p-benzoquinone; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / 1 h / 20 °C
4.1: p-benzoquinone; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 18 h / 80 °C / Schlenk technique
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C
6.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 4 h / 20 °C
6.2: 1 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; triethylsilane; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; p-benzoquinone;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jacs.5b03570
