4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate

Base Information

• Chemical Name: 4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate
• CAS No.: 1046357-36-1
• Molecular Formula: C₂₅H₂₉N₃O₁₂
• Molecular Weight: 563.518

Synonyms:4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate

Chemical Property of 4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate

Chemical Property:

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Technology Process of 4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate

There total 1 articles about 4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-4-(nitrooxy)butyl 2-(tert-butoxycarbonylamino)-3-(4-hydroxyphenyl)propanoate (1046357-16-7) + 4-Nitrophenyl chloroformate (7693-46-1) → 4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate (1046357-36-1)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; for 21.1667h;

Reference yield:

4-nitrooxy-butyl (S)-2-(tert-butoxycarbonylamino)-3-(4-((4-nitrophenoxy)carbonyloxy)phenyl)propanoate (1046357-36-1) + triamcinolone acetonide (76-25-5,911437-91-7) → (2S)-4-nitrooxy-butyl 2-(tert-butoxycarbonylamino)-3-(4-((2-((9R,10S,11S,13S,16R,17S)-9-fluoro-11-hydroxy-16,17-((1-methylethylidene)bis(oxy))-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxo-ethoxy)carbonyloxy)phenyl)propanoate (1046357-40-7)

Guidance literature:

With dmap; scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 - 20 ℃; for 70h;

upstream raw materials:

(S)-4-(nitrooxy)butyl 2-(tert-butoxycarbonylamino)-3-(4-hydroxyphenyl)propanoate

4-Nitrophenyl chloroformate

Downstream raw materials:

(2S)-4-nitrooxy-butyl 2-(tert-butoxycarbonylamino)-3-(4-((2-((9R,10S,11S,13S,16R,17S)-9-fluoro-11-hydroxy-16,17-((1-methylethylidene)bis(oxy))-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxo-ethoxy)carbonyloxy)phenyl)propanoate

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