(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Base Information

Chemical Name:(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene
CAS No.:134269-52-6
Molecular Formula:C₁₅H₉F₁₃
Molecular Weight:436.216
Hs Code.:

Synonyms:(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

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Technology Process of (E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

There total 5 articles about (E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1866-39-3,940-61-4
4-methylcinnamic acid

: 355-43-1
n-perfluorohexyl iodide

: 134269-52-6
(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With [2,2]bipyridinyl; copper(I) trifluoromethanesolfonate toluene complex; Dimethyl phosphite; In acetonitrile; at 80 ℃; for 72h; stereoselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.6b02613

Reference yield: 76.0%

: 1866-39-3,940-61-4
4-methylcinnamic acid

: 335-56-8
1-bromo-1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluorohexane

: 134269-52-6
(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With [2,2]bipyridinyl; copper(I) trifluoromethanesolfonate toluene complex; Dimethyl phosphite; In acetonitrile; at 80 ℃; for 72h; stereoselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.6b02613

Reference yield:

: 624-31-7
4-tolyl iodide

: 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

: 1423439-43-3
C₁₅H₉F₁₃

: 134269-52-6
(E)-1-methyl-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With potassium phosphate; C₃₀H₂₅ClN₂P₂Pd; In N,N-dimethyl-formamide; at 110 ℃; for 24h; Overall yield = 89 %; Sealed tube;
DOI:10.1016/j.jfluchem.2012.12.009