alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate

Base Information

Chemical Name:alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate
CAS No.:65530-21-4
Molecular Formula:C₁₆H₂₂O₁₀S₂
Molecular Weight:438.477
Hs Code.:
DSSTox Substance ID:DTXSID501133772

Synonyms:65530-21-4;DTXSID501133772;|A-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate;alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate

Suppliers and Price of alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate

Chemical Property:

XLogP3:0.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:6
Exact Mass:438.06543924
Heavy Atom Count:28
Complexity:720

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1C(C(C2C(O1)COC(O2)C3=CC=CC=C3)OS(=O)(=O)C)OS(=O)(=O)C
Isomeric SMILES:CO[C@@H]1[C@@H]([C@H]([C@H]2[C@H](O1)CO[C@H](O2)C3=CC=CC=C3)OS(=O)(=O)C)OS(=O)(=O)C

Technology Process of alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate

There total 6 articles about alpha-D-Glucopyranoside, methyl 4,6-O-[(R)-phenylmethylene]-, 2,3-dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124-63-0
methanesulfonyl chloride

: 3162-96-7
4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside

: 65530-21-4
methyl 4,6-O-benzylidene-2,3-di-O-methanesulfonyl-α-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1016/j.tetlet.2003.12.034

Reference yield: 81.0%

: 79549-74-9
methyl 4,6-O-benzylidene-α-D-allopyranoside

: 124-63-0
methanesulfonyl chloride

: 6619-12-1,18929-72-1,23819-27-4,23819-32-1,24017-81-0,26532-07-0,26540-58-9,65530-21-4,65530-23-6
methyl 4,6-O-benzylidene-2,3-O-p-methanesulfonyl-α-D-gluco-pyranoside

Guidance literature:: In pyridine; for 24h; Ambient temperature;
DOI:10.1139/v82-050

Reference yield: 67.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 124-63-0
methanesulfonyl chloride

: 1824-94-8
methyl beta-D-galactopyranoside

: 6619-12-1,18929-72-1,23819-27-4,23819-32-1,24017-81-0,26532-07-0,26540-58-9,65530-21-4,65530-23-6
Methyl-4,6-benzyliden-2,3-di-O-mesyl-β-D-galactosid

Guidance literature:: benzaldehyde dimethyl acetal; methyl beta-D-galactopyranoside; With camphor-10-sulfonic acid; In N,N-dimethyl-formamide;

methanesulfonyl chloride; With pyridine;
DOI:10.1021/jo300764k