(2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate

Base Information

• Chemical Name: (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate
• CAS No.: 1228187-14-1
• Molecular Formula: C₃₆H₅₄N₂O₅SSi
• Molecular Weight: 654.987

Synonyms:(2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate

Chemical Property of (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate

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Technology Process of (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate

There total 1 articles about (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C32H52O5Si (1228187-22-1) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate (1228187-14-1)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 8h;

DOI:10.1021/ol100513y

Reference yield: 83.0%

(2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-(O-methoxy-1H-imidazol-1-carbothioyl)furan-2-carboxylate (1228187-14-1) → (2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-methylfuran-2-carboxylate (1228187-18-5)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; at 85 ℃; for 1.25h;

DOI:10.1021/ol100513y

upstream raw materials:

C₃₂H₅₂O₅Si

1,1'-Thiocarbonyldiimidazole

Downstream raw materials:

(2S,5R)-((1S,2R)-2-(2-phenylpropan-2-yl)cyclohexyl)tetrahydro-5-((S)-2-trimethylsiloxy-6-methylhept-5-en-2-yl)-2-methylfuran-2-carboxylate

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