C₃₃H₃₈O₇

Base Information

Chemical Name:C₃₃H₃₈O₇
CAS No.:1354747-39-9
Molecular Formula:C₃₃H₃₈O₇
Molecular Weight:546.661
Hs Code.:

C<sub>33</sub>H<sub>38</sub>O<sub>7</sub>

Synonyms:C₃₃H₃₈O₇

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Chemical Property of C₃₃H₃₈O₇

Chemical Property:

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Technology Process of C₃₃H₃₈O₇

There total 7 articles about C₃₃H₃₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354747-41-3
C₃₁H₃₆O₅

: 64-19-7,77671-22-8
acetic acid

: 1354747-39-9
C₃₃H₃₈O₇

Guidance literature:: acetic acid; With tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone; In dichloromethane; at 55 ℃; for 0.0833333h; Inert atmosphere; Molecular sieve;

C₃₁H₃₆O₅; In dichloromethane; at 55 ℃; for 48h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol2032448

Reference yield:

: 201279-58-5
1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

: 1354747-39-9
C₃₃H₃₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; sodium methylate / 1 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

6.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

With 1H-imidazole; methanol; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); tetrabutyl ammonium fluoride; sodium methylate; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol2032448

Reference yield:

: 1354747-40-2
C₁₈H₃₆O₅Si

: 1354747-39-9
C₃₃H₃₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

4.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

With tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); tetrabutyl ammonium fluoride; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol2032448