benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

Base Information

Chemical Name:benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate
CAS No.:1262675-48-8
Molecular Formula:C₂₂H₂₄IN₃O₄
Molecular Weight:521.355
Hs Code.:

Synonyms:benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

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Chemical Property of benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

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Technology Process of benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

There total 4 articles about benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1005348-16-2
N-(3,3-dimethylallyl)-N'-N-bis-Cbz-guanidine

: 1262675-43-3
C₂₂H₂₄IN₃O₄

: 1262675-48-8
benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

Guidance literature:: With iodine; potassium carbonate; In acetonitrile; at -15 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2014.03.087

Reference yield:

: 1262675-43-3
C₂₂H₂₄IN₃O₄

: 1262675-48-8
benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2010.10.050

Reference yield:

: 1005348-16-2
N-(3,3-dimethylallyl)-N'-N-bis-Cbz-guanidine

: 1262675-48-8
benzyl 2-(((benzyloxy)carbonyl)imino)-4-(iodomethyl)-5,5-dimethylimidazolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; potassium carbonate / acetonitrile / -15 - 20 °C

2: potassium carbonate / acetonitrile / 16 h / 20 °C

With iodine; potassium carbonate; In acetonitrile;
DOI:10.1016/j.tetlet.2010.10.050