4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

Base Information

Chemical Name:4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol
CAS No.:306776-36-3
Molecular Formula:C₂₄H₄₈N₂O₂S₂
Molecular Weight:460.789
Hs Code.:

Synonyms:4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

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Chemical Property of 4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

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Technology Process of 4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

There total 1 articles about 4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 306776-71-6
4-[(1-{1-[(4-hydroxy-butylamino)-methyl]-cyclohexyldisulfanyl}-cyclohexylmethyl)-amino]-butan-1-ol

: 306776-36-3
4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

Guidance literature:: formaldehyd; 4-[(1-{1-[(4-hydroxy-butylamino)-methyl]-cyclohexyldisulfanyl}-cyclohexylmethyl)-amino]-butan-1-ol; In methanol; water; at 20 ℃; for 12h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jm000178w

Reference yield:

: 306776-36-3
4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

: 306776-40-9
4-[(1-mercapto-cyclohexylmethyl)-methyl-amino]-butan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jm000178w

Reference yield:

: 306776-36-3
4-{[1-(1-{[(4-hydroxy-butyl)-methyl-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-methyl-amino}-butan-1-ol

: 306776-46-5
C₁₂H₂₄N₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

2: 16 percent / t-BuONO; conc. HCl / ethanol / 0.25 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; tert.-butylnitrite; In tetrahydrofuran; ethanol; 1: Reduction / 2: Nitrosation;
DOI:10.1021/jm000178w