C₇₄H₁₁₀N₂₀O₁₆S

Base Information

• Chemical Name: C₇₄H₁₁₀N₂₀O₁₆S
• CAS No.: 252570-76-6
• Molecular Formula: C₇₄H₁₁₀N₂₀O₁₆S
• Molecular Weight: 1567.88
• Mol file: 252570-76-6.mol

Synonyms:C₇₄H₁₁₀N₂₀O₁₆S

Chemical Property of C₇₄H₁₁₀N₂₀O₁₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₇₄H₁₁₀N₂₀O₁₆S

There total 1 articles about C₇₄H₁₁₀N₂₀O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-L-Lys(Boc)-OPfp (86060-98-2) + (9H-fluoren-9-yl-methoxy)carbonyl-L-alanine pentafluorophenyl ester (86060-86-8) + Fmoc-Gly-OPfp (86060-85-7) + Fmoc-Tyr(tBu)-OPfp (86060-93-7) + Fmoc-Gln(Trt)-OPfp (132388-65-9) + Fmoc-L-proline pentafluorophenyl ester (125281-38-1,86060-90-4) + N-(9-fluorenylmethoxycarbonyl)-L-leucine pentafluorophenyl ester (86060-88-0) + N-α-Fmoc-L-methionine pentafluorophenyl ester (86060-94-8,210473-10-2) + 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-(1-trityl-1H-imidazol-4-yl)-propionic acid pentafluorophenyl ester + 3-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-2-pentafluorophenyloxycarbonyl-ethyl]-indole-1-carboxylic acid tert-butyl ester (181311-44-4) → C74H110N20O16S (252570-76-6)

Guidance literature:

Fmoc-Tyr(tBu)-OPfp; With benzotriazol-1-ol; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 3h;

With piperidine; In N,N-dimethyl-formamide; for 0.166667h;

Fmoc-L-Lys(Boc)-OPfp; (9H-fluoren-9-yl-methoxy)carbonyl-L-alanine pentafluorophenyl ester; Fmoc-Gly-OPfp; Fmoc-Gln(Trt)-OPfp; Fmoc-L-proline pentafluorophenyl ester; N-(9-fluorenylmethoxycarbonyl)-L-leucine pentafluorophenyl ester; N-α-Fmoc-L-methionine pentafluorophenyl ester; 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-(1-trityl-1H-imidazol-4-yl)-propionic acid pentafluorophenyl ester; 3-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-2-pentafluorophenyloxycarbonyl-ethyl]-indole-1-carboxylic acid tert-butyl ester; Further stages;

DOI:10.5012/bkcs.2013.34.2.549

upstream raw materials:

Fmoc-L-Lys(Boc)-OPfp

(9H-fluoren-9-yl-methoxy)carbonyl-L-alanine pentafluorophenyl ester

Fmoc-Gly-OPfp

Fmoc-Tyr(tBu)-OPfp

Refernces