2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

Base Information

Chemical Name:2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide
CAS No.:176646-55-2
Molecular Formula:C₁₄H₂₀O₂SSi
Molecular Weight:280.463
Hs Code.:

Synonyms:2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

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Chemical Property of 2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

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Technology Process of 2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

There total 3 articles about 2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 162318-37-8
2-(dimethylphenylsilyl)-thiacyclo hept-2-ene

: 176646-55-2
2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

Guidance literature:: With potassium peroxomonosulfate; In methanol; for 5h; Ambient temperature;
DOI:10.1016/0040-4020(96)00148-2

Reference yield:

: 147752-76-9
6-bromohexanoyl dimethylphenyl silane

: 176646-55-2
2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: HCl, H₂S / diethyl ether / -30 °C

2: 78 percent / NaOH / diethyl ether / Ambient temperature

3: 97 percent / KHSO₅ / methanol / 5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; potassium peroxomonosulfate; hydrogen sulfide; In methanol; diethyl ether;
DOI:10.1016/0040-4020(96)00148-2

Reference yield:

: 176646-52-9
6-bromo-1-dimethylphenylsilyl-1,1-hexane dithiol

: 176646-55-2
2-dimethylphenylsilyl-thiacyclo hept-2-ene S,S-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaOH / diethyl ether / Ambient temperature

2: 97 percent / KHSO₅ / methanol / 5 h / Ambient temperature

With sodium hydroxide; potassium peroxomonosulfate; In methanol; diethyl ether;
DOI:10.1016/0040-4020(96)00148-2