N-benzyl-2-bromo-5-methylbenzamide

Base Information

Chemical Name:N-benzyl-2-bromo-5-methylbenzamide
CAS No.:1401880-57-6
Molecular Formula:C₁₅H₁₄BrNO
Molecular Weight:304.186
Hs Code.:

Synonyms:N-benzyl-2-bromo-5-methylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2-bromo-5-methylbenzamide

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Technology Process of N-benzyl-2-bromo-5-methylbenzamide

There total 1 articles about N-benzyl-2-bromo-5-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 6967-82-4
2-bromo-5-methylbenzoic acid

: 100-46-9
benzylamine

: 1401880-57-6
N-benzyl-2-bromo-5-methylbenzamide

Guidance literature:: 2-bromo-5-methylbenzoic acid; With triethylamine; isobutyl chloroformate; In dichloromethane; for 0.25h; Inert atmosphere; Schlenk technique;

benzylamine; In dichloromethane; at 0 ℃;
DOI:10.1002/ejoc.201501170

Reference yield: 79.0%

: 1401880-57-6
N-benzyl-2-bromo-5-methylbenzamide

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1401880-77-0
5-benzyl-8-methylphenanthridin-6(5H)-one

Guidance literature:: With palladium diacetate; sodium carbonate; cesium fluoride; bis-diphenylphosphinomethane; In toluene; acetonitrile; at 20 - 110 ℃;
DOI:10.1021/jo3016192

Reference yield: 47.0%

: 1401880-57-6
N-benzyl-2-bromo-5-methylbenzamide

: C₃₀H₂₆N₂O₂

Guidance literature:: With palladium(II) trifluoroacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 100 ℃; for 12h; regioselective reaction; Sealed tube;
DOI:10.1016/j.mcat.2021.111766