4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

Base Information

Chemical Name:4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol
CAS No.:898815-31-1
Molecular Formula:C₃₅H₅₀N₂O₁₅
Molecular Weight:738.786
Hs Code.:

Synonyms:4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

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Chemical Property of 4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

There total 10 articles about 4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 863892-15-3
4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

: 898815-31-1
4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1002/anie.200600312

Reference yield:

: 863892-02-8
1-O-(2-oxoethyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 898815-31-1
4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

2: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

3: 100 percent / H₂ / Pd/C / CH₂Cl₂; methanol / 3 h / 20 °C / 2068.59 Torr

4: 65 percent / triethylamine; HOBT; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / dimethylformamide / 22 h / 20 °C

5: 100 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂; methanol / 10 h / 20 °C

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600898

Reference yield:

: 863986-24-7
1-O-allyl-2,3:5,6-di-O-isopropylidene-scyllo-inositol

: 898815-31-1
4-O-{(2-N,N-dibenzylaminoethyl)-4'-O-[(methoxycarbonylmethyl)-scyllo-inositol]-1'-O-ethyl-1-O-methylamido}-scyllo-inositol

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / sodium bicarbonate; ozone; triphenylphosphine / CH₂Cl₂; methanol / 12 h / 20 °C

2: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

3: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

4: 100 percent / H₂ / Pd/C / CH₂Cl₂; methanol / 3 h / 20 °C / 2068.59 Torr

5: 65 percent / triethylamine; HOBT; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / dimethylformamide / 22 h / 20 °C

6: 100 percent / p-toluenesulfonic acid monohydrate / CH₂Cl₂; methanol / 10 h / 20 °C

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; benzotriazol-1-ol; toluene-4-sulfonic acid; ozone; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600898