4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

Base Information

Chemical Name:4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol
CAS No.:863892-15-3
Molecular Formula:C₄₇H₆₆N₂O₁₅
Molecular Weight:899.045
Hs Code.:

4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

Synonyms:4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

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Chemical Property of 4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

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Technology Process of 4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

There total 8 articles about 4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 863892-05-1
4-O-(2-aminoethyl)-1-O-(methoxycarbonylmethyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 863892-06-2
4-O-(2-N,N-dibenzylaminoethyl)-1-O-(methoxycarbonyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 863892-15-3
4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

Guidance literature:: With dmap; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200600312

Reference yield:

: 863892-02-8
1-O-(2-oxoethyl)-2,3:5,6-diisopropylidene-scyllo-inositol

: 863892-15-3
4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

2: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

3: 100 percent / H₂ / Pd/C / CH₂Cl₂; methanol / 3 h / 20 °C / 2068.59 Torr

4: 65 percent / triethylamine; HOBT; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / dimethylformamide / 22 h / 20 °C

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600898

Reference yield:

: 863986-24-7
1-O-allyl-2,3:5,6-di-O-isopropylidene-scyllo-inositol

: 863892-15-3
4-O-[(2-N,N-dibenzylaminoethyl)-4'-O-{(methoxycarbonylmethyl)-2',3':5',6'-di-O-isopropylidene-scyllo-inositol}-1'-O-ethyl-1-O-methylamido]-2,3:5,6-di-O-isopropylidene-schyllo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / sodium bicarbonate; ozone; triphenylphosphine / CH₂Cl₂; methanol / 12 h / 20 °C

2: 76 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 12 h / 20 °C

3: 94 percent / silver(I) oxide; tetrabutylammonium iodide / CH₂Cl₂ / 12 h / 20 °C

4: 100 percent / H₂ / Pd/C / CH₂Cl₂; methanol / 3 h / 20 °C / 2068.59 Torr

5: 65 percent / triethylamine; HOBT; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / dimethylformamide / 22 h / 20 °C

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; benzotriazol-1-ol; ozone; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600898