p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

Base Information

• Chemical Name: p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane
• CAS No.: 1428770-78-8
• Molecular Formula: C₇₅H₈₇N₃O₅Si₄
• Molecular Weight: 1222.87

Synonyms:p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

Chemical Property of p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

Chemical Property:

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Technology Process of p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

There total 1 articles about p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

p-bromophenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane (1428770-77-7) + 4′-nitroazobenzene-4-boronic acid pinacol ester (1428770-73-3) → p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane (1428770-78-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; at 100 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.tet.2013.02.054

Reference yield: 89.0%

p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane (1428770-78-8) → p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane (1428770-79-9)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 28h;

DOI:10.1016/j.tet.2013.02.054

upstream raw materials:

p-bromophenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

4′-nitroazobenzene-4-boronic acid pinacol ester

Downstream raw materials:

p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

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