p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

Base Information

Chemical Name:p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane
CAS No.:1428770-79-9
Molecular Formula:C₅₇H₄₅N₃O₅Si
Molecular Weight:880.087
Hs Code.:

Synonyms:p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

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Technology Process of p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

There total 1 articles about p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1428770-78-8
p-(4-(4′nitroazobenzene))phenyl tri(3′-tert-butyldimethylsilyloxymethyl[4,1′]biphenyl)silane

: 1428770-79-9
p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 28h;
DOI:10.1016/j.tet.2013.02.054

Reference yield: 17.0%

: 1428770-79-9
p-(4-(4′-nitroazobenzene))phenyl tri(3′-hydroxymethyl[4,1′]biphenyl)silane

: 507-09-5
tiolacetic acid

: 1428770-76-6
p-(4-(4′-nitroazobenzene))phenyl tri(3′-thioacetyloxymethyl[4,1′]biphenyl)silane

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 4.5h;
DOI:10.1016/j.tet.2013.02.054