(4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

Base Information

Chemical Name:(4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate
CAS No.:1198118-27-2
Molecular Formula:C₁₄H₁₇NO₄S
Molecular Weight:295.359
Hs Code.:

Synonyms:(4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

Chemical Property:

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Technology Process of (4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

There total 2 articles about (4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26349-74-6,26349-75-7,58526-55-9,21055-39-0
2-isothiocyanatopropionic acid methyl ester

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1198118-27-2
(4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

: C₁₄H₁₇NO₄S

: C₁₄H₁₇NO₄S

Guidance literature:: With C₃₆H₂₈N₂O₄; dibutylmagnesium; In tetrahydrofuran; n-heptane; toluene; at 20 ℃; for 48h; optical yield given as %ee; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja908571w

Reference yield:

: 26349-74-6,26349-75-7,58526-55-9,21055-39-0
2-isothiocyanatopropionic acid methyl ester

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1198118-27-2
(4R,5R)-methyl 5-(4-methoxyphenyl)-4,5-dimethyl-2-thioxooxazolidine-4-carboxylate

: C₁₄H₁₇NO₄S

: C₁₄H₁₇NO₄S

Guidance literature:: With C₃₆H₂₈N₂O₄; dibutylmagnesium; In toluene; at 20 ℃; for 48h; optical yield given as %ee; enantioselective reaction; Molecular sieve;
DOI:10.1002/tcr.201100020