1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide

Base Information

• Chemical Name: 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide
• CAS No.: 111601-95-7
• Molecular Formula: C₃₁H₄₀O₅
• Molecular Weight: 492.656
• Mol file: 111601-95-7.mol

Synonyms:1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide

Chemical Property of 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide

There total 2 articles about 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

p-Phenylisopropylperoxyisopropylhydroperoxyisopropylbenzol (57321-13-8) + 1-(1-methyl-1-hydroxyethyl)-4-hydroxymethylbenzene (88416-58-4) → 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide (111601-95-7)

Guidance literature:

With perchloric acid; In acetic acid; at 20 ℃; for 3h;

Reference yield:

4’-(acetoxymethyl)acetophenone (95827-11-5) → 1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide (111601-95-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / diethyl ether / 4 h / 0 - 5 °C

2: 64 percent / perchloric acid / acetic acid / 3 h / 20 °C

With perchloric acid; In diethyl ether; acetic acid;

Reference yield:

1-methyl-1-(4-hydroxymethylphenyl)ethyl 1-methyl-1-<4-<1-methyl-1-(1-methyl-1-phenylethylperoxy)ethyl>phenyl>ethyl peroxide (111601-95-7) → 4-[1-Methyl-1-(1-methyl-1-{4-[1-methyl-1-(1-methyl-1-phenyl-ethylperoxy)-ethyl]-phenyl}-ethylperoxy)-ethyl]-benzoic acid (73676-93-4)

Guidance literature:

With potassium permanganate; In water; ethyl acetate; at 20 - 25 ℃; for 4h;

upstream raw materials:

p-Phenylisopropylperoxyisopropylhydroperoxyisopropylbenzol

1-(1-methyl-1-hydroxyethyl)-4-hydroxymethylbenzene

4’-(acetoxymethyl)acetophenone

Downstream raw materials:

4-[1-Methyl-1-(1-methyl-1-{4-[1-methyl-1-(1-methyl-1-phenyl-ethylperoxy)-ethyl]-phenyl}-ethylperoxy)-ethyl]-benzoic acid