6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline

Base Information

• Chemical Name: 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline
• CAS No.: 185104-71-6
• Molecular Formula: C₄₁H₄₃NO₅
• Molecular Weight: 629.796

Synonyms:6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline

Chemical Property of 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline

Chemical Property:

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Technology Process of 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline

There total 3 articles about 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[6,7-Bis-benzyloxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-phenyl-ethanone (185104-69-2) → 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline (185104-71-6)

Guidance literature:

With borane-THF; In tetrahydrofuran; for 2.5h; Heating;

DOI:10.1021/jm950896w

Reference yield:

1-(3,4,5-trimethoxybenzyl)-6,7-bis(benzyloxy)-1,2,3,4-tetrahydroisoquinoline (102921-08-4) → 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline (185104-71-6)

Guidance literature:

Multi-step reaction with 2 steps

1: MgSO₄, Na₂CO₃ / a) CH₂Cl₂, 15 min, b) CH₂Cl₂, RT, 30 min

2: BH₃*THF / tetrahydrofuran / 2.5 h / Heating

With borane-THF; sodium carbonate; magnesium sulfate; In tetrahydrofuran;

DOI:10.1021/jm950896w

Reference yield:

phenylacetyl chloride (103-80-0) → 6,7-Bis-benzyloxy-2-phenethyl-1-(3,4,5-trimethoxy-benzyl)-1,2,3,4-tetrahydro-isoquinoline (185104-71-6)

Guidance literature:

Multi-step reaction with 2 steps

1: MgSO₄, Na₂CO₃ / a) CH₂Cl₂, 15 min, b) CH₂Cl₂, RT, 30 min

2: BH₃*THF / tetrahydrofuran / 2.5 h / Heating

With borane-THF; sodium carbonate; magnesium sulfate; In tetrahydrofuran;

DOI:10.1021/jm950896w

upstream raw materials:

1-[6,7-Bis-benzyloxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-phenyl-ethanone

1-(3,4,5-trimethoxybenzyl)-6,7-bis(benzyloxy)-1,2,3,4-tetrahydroisoquinoline

phenylacetyl chloride

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