allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Base Information

Chemical Name:allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside
CAS No.:88862-56-0
Molecular Formula:C₆₄H₆₄O₁₃
Molecular Weight:1041.2
Hs Code.:

Synonyms:allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Chemical Property of allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

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Technology Process of allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

There total 1 articles about allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 61236-87-1
allyl 2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 81713-25-9
2,3-di-O-benzoyl-4,6-di-O-benzyl-α-D-galactopyranosyl chloride

: 88862-56-0
allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane;
DOI:10.1016/0008-6215(86)80014-3

Reference yield:

: 88862-56-0
allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 106238-74-8,106238-89-5
O-(4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 0.13M sodium methoxide / methanol / 2 h / Ambient temperature

2: 1,4-diazabicyclo <2.2.2.> octane / tris (triphenylphosphine) rhodium(I)chloride / ethanol; H₂O / 6 h / Heating

3: HgO, HgCl₂ / acetone; H₂O / 0.5 h

With 1,4-diaza-bicyclo[2.2.2]octane; sodium methylate; mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In methanol; ethanol; water; acetone;
DOI:10.1016/0008-6215(86)80014-3

Reference yield:

: 88862-56-0
allyl O-(2,3-di-O-benzoyl-4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 107333-59-5
1-propenyl O(4,6-di-O-benzyl-β-D-galactopyranosyl)-(1<*>3)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 0.13M sodium methoxide / methanol / 2 h / Ambient temperature

2: 1,4-diazabicyclo <2.2.2.> octane / tris (triphenylphosphine) rhodium(I)chloride / ethanol; H₂O / 6 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; sodium methylate; Wilkinson's catalyst; In methanol; ethanol; water;
DOI:10.1016/0008-6215(86)80014-3