C₁₃H₁₃IN₂O

Base Information

• Chemical Name: C₁₃H₁₃IN₂O
• CAS No.: 1219010-34-0
• Molecular Formula: C₁₃H₁₃IN₂O
• Molecular Weight: 340.164
• Mol file: 1219010-34-0.mol

Synonyms:C₁₃H₁₃IN₂O

Chemical Property of C₁₃H₁₃IN₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₃IN₂O

There total 1 articles about C₁₃H₁₃IN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C6H9IN2 (1219010-52-2) + benzoyl chloride (98-88-4) → C13H13IN2O (1219010-34-0)

Guidance literature:

With sodium hydride; In dichloromethane; mineral oil; at 0 - 20 ℃; for 1.25h; Inert atmosphere;

DOI:10.1021/ja910653k

Reference yield: 45.0%

C13H13IN2O (1219010-34-0) → N-cyano-N-(pent-4-en-1-yl)benzamide (1219010-36-2) + C13H12N2O (1219010-35-1) + 6-methyl-6,7,8,9-tetrahydro-11H-pyrido[2,1-b]quinazolin-11-one (959050-41-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Inert atmosphere; Reflux;

DOI:10.1021/ja910653k

upstream raw materials:

C₆H₉IN₂

benzoyl chloride

Downstream raw materials:

N-cyano-N-(pent-4-en-1-yl)benzamide

C₁₃H₁₂N₂O

6-methyl-6,7,8,9-tetrahydro-11H-pyrido[2,1-b]quinazolin-11-one