Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

Base Information

Chemical Name:Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate
CAS No.:118128-96-4
Molecular Formula:C₂₀H₁₈N₄O₄
Molecular Weight:378.387
Hs Code.:

Synonyms:Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

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Chemical Property of Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

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Technology Process of Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

There total 4 articles about Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105-56-6
ethyl 2-cyanoacetate

: 118128-92-0
Ethyl 4-amino-5-cyano-6-phenyl-2-trichloromethyl-3-pyridinecarboxylate

: 118128-96-4
Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

Guidance literature:: With sodium; In 1,4-dioxane; for 5h; Heating;
DOI:10.1002/ardp.19883210919

Reference yield:

: 614-16-4
Benzoylacetonitrile

: 118128-96-4
Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / CHCl₃ / 1 h / Heating

2: 75 percent / sodium acetate / ethanol

3: 70 percent / Na / dioxane / 5 h / Heating

With sodium acetate; sodium; triethylamine; In 1,4-dioxane; ethanol; chloroform;
DOI:10.1002/ardp.19883210919

Reference yield:

: 27317-59-5
Ethyl 3-ethoxy-3-iminopropionate

: 118128-96-4
Ethyl 2-(4-amino-5-cyano-3-ethoxycarbonyl-6-phenylpyridine-2-yl)-cyanoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / CHCl₃ / 1 h / Heating

2: 75 percent / sodium acetate / ethanol

3: 70 percent / Na / dioxane / 5 h / Heating

With sodium acetate; sodium; triethylamine; In 1,4-dioxane; ethanol; chloroform;
DOI:10.1002/ardp.19883210919