(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

Base Information

Chemical Name:(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline
CAS No.:1089681-69-5
Molecular Formula:C₁₈H₁₇NO₂
Molecular Weight:279.338
Hs Code.:

Synonyms:(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

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Chemical Property of (E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

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Technology Process of (E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

There total 9 articles about (E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10541-83-0,937737-33-2
N-methyl-p-aminobenzoic acid

: 1089681-69-5
(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetyl chloride / 20 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 °C

3.1: water; 1,4-dioxane / 16 h / 20 °C

4.1: sulfur trioxide pyridine complex; triethylamine; dimethyl sulfoxide / 3 h / 0 - 20 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C

5.2: 4.5 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; acetyl chloride; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 1462470-22-9
((6-methoxybenzofuran-2-yl)methyl)triphenylphosphonium bromide

: 1089681-69-5
(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C

1.2: 4.5 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C

With sodium hexamethyldisilazane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 181819-75-0
(4-(methylamino)phenyl)methanol

: 1089681-69-5
(E)-4-(2-(6-methoxybenzofuran-2-yl)vinyl)-N-methylaniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; 1,4-dioxane / 16 h / 20 °C

2.1: sulfur trioxide pyridine complex; triethylamine; dimethyl sulfoxide / 3 h / 0 - 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C

3.2: 4.5 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 24 h / 0 - 20 °C

With sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;