methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Base Information

Chemical Name:methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate
CAS No.:1355371-20-8
Molecular Formula:C₂₅H₂₅NO₃
Molecular Weight:387.478
Hs Code.:

Synonyms:methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

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Chemical Property of methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Chemical Property:

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Technology Process of methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

There total 4 articles about methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1355371-10-6
methyl 7-(3-aminophenoxy)-1,2,3,4-tetrahydronaphthalene-2-carboxylate hydrochloride

: 100-52-7
benzaldehyde

: 1355371-20-8
methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Guidance literature:: methyl 7-(3-aminophenoxy)-1,2,3,4-tetrahydronaphthalene-2-carboxylate hydrochloride; benzaldehyde; With triethylamine; In methanol; at 20 ℃; for 1h;

With sodium cyanoborohydride; acetic acid; In methanol; pH=7;

Reference yield:

: 31846-36-3
7-hydroxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid

: 1355371-20-8
methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / Reflux

2.1: triethylamine / copper diacetate / dichloromethane / 20 °C / 4 ? Molecular sieve

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 4 h / 20 °C

4.1: triethylamine / methanol / 1 h / 20 °C

4.2: pH 7

With hydrogenchloride; sulfuric acid; triethylamine; copper diacetate; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: methyl 7-hydroxy-1,2,3,4-tetrahydronaphtha-lene-2-carboxylate

: 1355371-20-8
methyl 7-[3-(benzylamino)phenoxy]-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / copper diacetate / dichloromethane / 20 °C / 4 ? Molecular sieve

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 4 h / 20 °C

3.1: triethylamine / methanol / 1 h / 20 °C

3.2: pH 7

With hydrogenchloride; triethylamine; copper diacetate; In 1,4-dioxane; methanol; dichloromethane;