ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

Base Information

Chemical Name:ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate
CAS No.:1581259-17-7
Molecular Formula:C₁₇H₁₆ClN₃O₅S
Molecular Weight:409.85
Hs Code.:

Synonyms:ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

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Chemical Property of ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

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Technology Process of ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

There total 2 articles about ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1581259-58-6
ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]acetate

: 1581259-17-7
ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

Guidance literature:: With 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 0 ℃; for 0.266667h; Sealed tube;
DOI:10.1039/c4cc00250d

Reference yield:

: 41018-73-9
4-chloro-N-(4-methoxyphenyl)aniline

: 1581259-17-7
ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 24 h / 20 °C

2: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.27 h / 0 °C / Sealed tube

With 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.1039/c4cc00250d

Reference yield: 34.0%

: 1581259-17-7
ethyl 2-[N-(4-chlorophenyl)-N-(4-methoxyphenyl)sulfamoyl]-2-diazoacetate

: 1581259-35-9
ethyl 5-chloro-1-(4-methoxyphenyl)-1,3-dihydrobenzo[c]isothiazole-3-carboxylate 2,2-dioxide

: 1581259-37-1
ethyl 1-(4-chlorophenyl)-5-methoxy-1,3-dihydrobenzo[c]isothiazole-3-carboxylate 2,2-dioxide

Guidance literature:: With rhodium (II) octanoate dimer; In 1,2-dichloro-ethane; for 2h; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1039/c4cc00250d