2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

Base Information

Chemical Name:2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide
CAS No.:1198785-31-7
Molecular Formula:C₁₉H₂₆F₃NO₂Si
Molecular Weight:385.502
Hs Code.:

Synonyms:2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

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Chemical Property of 2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

Chemical Property:

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Technology Process of 2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

There total 11 articles about 2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₄ClF₃O₂Si

: 1198785-31-7
2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 0.25h;
DOI:10.1021/ml500387y

Reference yield:

: 1198785-60-2
4-(2-[1,3]dioxan-2-ylphenyl)-1,1,1-trifluoro-4-methylpentan-2-one

: 1198785-31-7
2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: aluminium; mercury dichloride / tetrahydrofuran / 1 h / 50 °C

1.2: 2 h / -78 - 20 °C

2.1: hydrogenchloride / tetrahydrofuran; water / 16 h / 40 °C

3.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 16 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: thionyl chloride; pyridine / dichloromethane / 0.25 h / 20 °C

6.1: ammonia / methanol / 0.25 h / 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; ammonia; aluminium; mercury dichloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ml500387y

Reference yield:

: 1198785-30-6
2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxy-hex-5-ynyl)benzoic acid

: 1198785-31-7
2-(1,1-dimethyl-3-trifluoromethyl-3-trimethylsilanyloxyhex-5-ynyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; pyridine / dichloromethane / 0.25 h / 20 °C

2: ammonia / methanol / 0.25 h / 20 °C

With pyridine; thionyl chloride; ammonia; In methanol; dichloromethane;
DOI:10.1021/ml500387y