3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

Base Information

Chemical Name:3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride
CAS No.:1597602-07-7
Molecular Formula:C₂₅H₂₆BrN₂*Cl
Molecular Weight:469.852
Hs Code.:

Synonyms:3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

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Chemical Property of 3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

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Technology Process of 3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

There total 5 articles about 3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1597602-52-2
3-bromo-5-(hex-1’-yl)-6-phenyl-8-nitrophenanthridinium chloride

: 1597602-07-7
3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

Guidance literature:: With iron; In ethanol; acetic acid; at 40 ℃; for 1.5h;
DOI:10.1002/chem.201304241

Reference yield:

: 403615-35-0
1-(2-iodo-5-nitro-phenyl)-1-phenyl-methanone

: 1597602-07-7
3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; N-ethyl-N,N-diisopropylamine / ethanol / 22 h / Inert atmosphere; Reflux

2: titanium tetrachloride / toluene / 35 h / 0 - 20 °C / Inert atmosphere

3: tetrahydrofuran / 2 h / 100 °C / Inert atmosphere; Sealed tube; Microwave irradiation

4: iron / acetic acid; ethanol / 1.5 h / 40 °C

With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; titanium tetrachloride; iron; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetic acid; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1002/chem.201304241

Reference yield:

: 216393-64-5
(4-bromo-2-fluorophenyl)boronic acid

: 1597602-07-7
3-bromo-5-(hex-1’-yl)-6-phenyl-8-aminophenanthridinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; N-ethyl-N,N-diisopropylamine / ethanol / 22 h / Inert atmosphere; Reflux

2: titanium tetrachloride / toluene / 35 h / 0 - 20 °C / Inert atmosphere

3: tetrahydrofuran / 2 h / 100 °C / Inert atmosphere; Sealed tube; Microwave irradiation

4: iron / acetic acid; ethanol / 1.5 h / 40 °C

With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; titanium tetrachloride; iron; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetic acid; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1002/chem.201304241