2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

Base Information

Chemical Name:2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide
CAS No.:700359-71-3
Molecular Formula:C₂₁H₂₆BrN₃O₄S
Molecular Weight:496.425
Hs Code.:

Synonyms:2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

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Chemical Property of 2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

Chemical Property:

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Technology Process of 2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

There total 4 articles about 2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-bromo-2-methoxy-4-[(2-piperidin-1-yl-benzylcarbamoyl)-methyl]-benzenesulfonyl chloride

: 700359-71-3
2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

Guidance literature:: With ammonia; In dichloromethane; at 0 ℃;
DOI:10.1081/SCC-120028635

Reference yield:

: 1798-09-0
m-methoxyphenylacetic acid

: 700359-71-3
2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / bromine / CH₂Cl₂ / 2 h / 20 °C

2: 62 percent / dicyclohexylcarbodiimide / toluene / 10 h / 20 °C

3: chlorosulfonic acid / CH₂Cl₂ / 5 h / Heating

4: NH₃ gas / CH₂Cl₂ / 0 °C

With chlorosulfonic acid; ammonia; bromine; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1081/SCC-120028635

Reference yield:

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 700359-71-3
2-(4-aminosulfonyl-2-bromo-5-methoxyphenyl)-N-(2-piperidinobenzyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / dicyclohexylcarbodiimide / toluene / 10 h / 20 °C

2: chlorosulfonic acid / CH₂Cl₂ / 5 h / Heating

3: NH₃ gas / CH₂Cl₂ / 0 °C

With chlorosulfonic acid; ammonia; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1081/SCC-120028635