2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

Base Information

Chemical Name:2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine
CAS No.:97980-49-9
Molecular Formula:C₁₆H₁₆N₂O₄S₃
Molecular Weight:396.512
Hs Code.:

2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ<sup>4</sup>-[1,2]thiazine

Synonyms:2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

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Technology Process of 2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

There total 3 articles about 2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 667-20-9
N,N'-bis(phenylsulfonyl)sulfur diimide

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: 97980-49-9
2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

Guidance literature:: In 1,2-dimethoxyethane; at 23 ℃; for 0.166667h; Solvent;
DOI:10.1039/c4sc01152j

Reference yield:

: 98-10-2
benzenesulfonamide

: 97980-49-9
2-benzenesulfonyl-1-benzenesulfonylimino-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / benzene / 72 h / 80 °C / Inert atmosphere

1.2: 12 h / 23 °C / Inert atmosphere

2.1: dichloromethane / 0.33 h / 23 °C / Sealed tube; Inert atmosphere

With thionyl chloride; In dichloromethane; benzene;
DOI:10.1002/anie.201701796