(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

Base Information

Chemical Name:(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine
CAS No.:914360-21-7
Molecular Formula:C₂₉H₄₁NO₂Se
Molecular Weight:514.61
Hs Code.:

Synonyms:(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

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Technology Process of (2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

There total 4 articles about (2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 914359-84-5
(1S,3S,6aS,9R,10aR,11aS)-1-phenyl-3-(1-methyl-1-phenylselenenylethyl)-6,6,9-trimethyl-decahydro-3H,7H-[1,4]oxazino[3,4-b][1,3]benzoxazine

: 914360-21-7
(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/jo061547k

Reference yield:

: 914359-71-0
(S)-[(2S,4aS,7R,8aR)-3-(3-methylbut-2-enyl)-4,4,7-trimethyl-octahydro-2H-benzo[e][1,3]oxazin-2-yl](phenyl)methanol

: 914360-21-7
(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂ / 5 h / 0 °C

2: 85 percent / LiAlH₄; AlCl₃ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo061547k

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 914360-21-7
(2S,6S)-4-(8-mentholyl)-2-(1-methyl-1-phenylselenenylethyl)-6-phenyl-morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂ / 5 h / 0 °C

2: 85 percent / LiAlH₄; AlCl₃ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo061547k