10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

Base Information

Chemical Name:10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan
CAS No.:113000-33-2
Molecular Formula:C₂₉H₄₂O₄S
Molecular Weight:486.716
Hs Code.:

Synonyms:10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

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Chemical Property of 10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

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Technology Process of 10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

There total 4 articles about 10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 882-33-7
diphenyldisulfane

: 113000-26-3
10-<2'-(Methoxymethoxy)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

: 113000-33-2
10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 113000-33-2
10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridinium-p-toluenesulfonate / CH₂Cl₂ / 3.5 h

2: 78 percent / 1.55 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

3: 93 percent / 1.55 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 53463-68-6
1-bromo-10-decanol

: 113000-33-2
10'-<2'-(Methoxymethoxy)-3'-(phenylthio)phenyl>-1-<(RS)-2-tetrahydropyranyloxy>decan

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridinium-p-toluenesulfonate / CH₂Cl₂ / 3.5 h

2: 78 percent / 1.55 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

3: 93 percent / 1.55 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;