(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:56650-22-7
Molecular Formula:C₂₄H₃₈O₁₀
Molecular Weight:486.56
Hs Code.:

Synonyms:(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 8 articles about (2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2216-51-5
(-)-menthol

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 56650-22-7
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With sulfonated graphene oxide; In neat (no solvent); at 80 ℃; for 6h; stereoselective reaction; Green chemistry;
DOI:10.1080/07328303.2015.1120874

Reference yield: 74.0%

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 56650-22-7
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With metal carbonates; In neat (no solvent); for 9h; Milling;
DOI:10.1016/j.carres.2013.06.018

Reference yield: 61.0%

: 100432-86-8
1-deoxy-1-[(R/S)-(phenyl)sulfinyl]-2,3,4,6-tetra-O-acetyl-β-D-glucopyranose

: 2216-51-5
(-)-menthol

: 56650-22-7
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With gold(III) chloride; silver trifluoromethanesulfonate; In dichloromethane; at 35 - 39 ℃; for 0.416667h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.carres.2016.11.012