(2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate

Base Information

Chemical Name:(2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate
CAS No.:1201668-14-5
Molecular Formula:C₄₁H₆₀O₆Si₂
Molecular Weight:705.095
Hs Code.:

Synonyms:(2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate

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Chemical Property of (2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate

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Technology Process of (2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate

There total 1 articles about (2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1201668-13-4
(2R,3S,4S)-5-[(1,1-dimethylethyl)diphenylsilyloxy]-2,4-dimethyl-3-(triethylsilyloxy)-pentanal

: 473758-96-2
C₆H₅CO₂CH(CH₃)C(C₂H₄)OB(C₆H₁₁)2

: 1201668-14-5
(2R,4S,5S,6S,7S,8S)-9-[(1,1-dimethylethyl)diphenylsilyloxy]-5-hydroxy-4,6,8-trimethyl-3-oxo-7-(triethylsilyloxy)nonan-2-yl benzoate

Guidance literature:: (2R,3S,4S)-5-[(1,1-dimethylethyl)diphenylsilyloxy]-2,4-dimethyl-3-(triethylsilyloxy)-pentanal; C₆H₅CO₂CH(CH₃)C(C₂H₄)OB(C₆H₁₁)2; In diethyl ether; at -78 - -25 ℃; for 13h; Inert atmosphere;

With water; dihydrogen peroxide; In methanol; diethyl ether; at 0 ℃; for 1h; pH=7; Inert atmosphere; buffer solution;
DOI:10.1002/anie.200904607