(S)-2-HYDROXYMETHYLCYCLOHEXANONE

Base Information

Chemical Name:(S)-2-HYDROXYMETHYLCYCLOHEXANONE
CAS No.:220199-90-6
Molecular Formula:C7H12 O2
Molecular Weight:128.171
Hs Code.:
Mol file:220199-90-6.mol

Synonyms:(S)-2-HYDROXYMETHYLCYCLOHEXANONE

Suppliers and Price of (S)-2-HYDROXYMETHYLCYCLOHEXANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(S)-2-HYDROXYMETHYL-CYCLOHEXANONE 95.00%
1G
$ 955.65

American Custom Chemicals Corporation
(S)-2-HYDROXYMETHYL-CYCLOHEXANONE 95.00%
0.25G
$ 490.00

Total 2 raw suppliers

Chemical Property of (S)-2-HYDROXYMETHYLCYCLOHEXANONE

Chemical Property:

PSA：37.30000
LogP:0.73800

Purity/Quality:: (S)-2-HYDROXYMETHYL-CYCLOHEXANONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-2-HYDROXYMETHYLCYCLOHEXANONE

There total 9 articles about (S)-2-HYDROXYMETHYLCYCLOHEXANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 220199-90-6
(S)-αlfa;-hydroxymethylcyclohexanone

Guidance literature:: formaldehyd; cyclohexanone; With L-threonine; magnesium sulfate; In tetrahydrofuran; water; at 20 ℃; for 120h; Sealed vial;

With water; ammonium chloride; In tetrahydrofuran; optical yield given as %ee; enantioselective reaction; Saturated solution;
DOI:10.1016/j.tet.2009.11.100

Reference yield: 37.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 75-07-0,9002-91-9
acetaldehyde

: 220199-90-6
(S)-αlfa;-hydroxymethylcyclohexanone

Guidance literature:: With water; (2S,4R)-4-((tert-butyldiphenylsilyl)oxy)pyrrolidine-2-carboxylic acid; at 20 ℃; for 90h;
DOI:10.1002/chem.200700363

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 220199-90-6
(S)-αlfa;-hydroxymethylcyclohexanone

: 784144-22-5
(R)-2-(hydroxymethyl)cyclohexanone

Guidance literature:: With water; (S, S)-6,6’-bis(1-hydroxy-2,2-dimethylpropyl)-2,2’-bipyridine; scandium tris(trifluoromethanesulfonate); In acetonitrile; at -20 ℃; for 34h; Title compound not separated from byproducts;
DOI:10.1021/ja047896i