Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

Base Information

Chemical Name:Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide
CAS No.:190660-00-5
Molecular Formula:C₁₆H₁₃ClN₂O₂S₃
Molecular Weight:396.942
Hs Code.:

Synonyms:Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

Suppliers and Price of Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

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Technology Process of Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

There total 2 articles about Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-15-8,11095-43-5
Benzo[b]thiophene

: 190660-00-5
Benzo[b]thiophene-2-sulfonic acid 1-(4-chloro-phenylamino)-1-methylsulfanyl-meth-(Z)-ylideneamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) hydroxylamine O-sulfonic acid, NaOAc / 1.) THF, hexane, reflux, 4 h, 2.) THF, hexane, RT, 8 h

2: 1.) aq. NaOH

With sodium hydroxide; n-butyllithium; sodium acetate; hydroxylamine-O-sulfonic acid;
DOI:10.1021/jm9607818