[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

Base Information

Chemical Name:[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester
CAS No.:932743-84-5
Molecular Formula:C₂₈H₃₁N₃O₈
Molecular Weight:537.569
Hs Code.:

Synonyms:[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

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Chemical Property of [1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

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Technology Process of [1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

There total 1 articles about [1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 6315-89-5
3,4-dimethoxyaniline

: 4515-23-5
N-benzyloxycarbonyl-L-aspartic acid anhydride

: 932743-84-5
[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/ol0700207

Reference yield: 92.0%

: 932743-84-5
[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

: 98-88-4
benzoyl chloride

: 932743-85-6
2-benzoylamino-N¹,N⁴-bis-(3,4-dimethoxy-phenyl)-succinamide

Guidance literature:: [1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester; With hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; at 20 ℃; for 4h;

benzoyl chloride; With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; for 1h;
DOI:10.1021/ol0700207

Reference yield:

: 932743-84-5
[1,2-bis-(3,4-dimethoxy-phenylcarbamoyl)-ethyl]-carbamic acid benzyl ester

: 932743-86-7
N²-benzyl-N¹,N⁴-bis-(3,4-dimethoxy-phenyl)-butane-1,2,4-triamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd/C / dimethylformamide; ethanol / 4 h / 20 °C

1.2: 92 percent / triethylamine / dimethylformamide; tetrahydrofuran / 1 h

2.1: 55 percent / NaBH₄; iodine / tetrahydrofuran / 12 h / Heating

With sodium tetrahydroborate; hydrogen; iodine; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol0700207