β-(m-Bromanilino)acrolein

Base Information

• Chemical Name: β-(m-Bromanilino)acrolein
• CAS No.: 51217-98-2
• Molecular Formula: C₉H₈BrNO
• Molecular Weight: 226.073
• Mol file: 51217-98-2.mol

Synonyms:β-(m-Bromanilino)acrolein

Chemical Property of β-(m-Bromanilino)acrolein

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of β-(m-Bromanilino)acrolein

There total 2 articles about β-(m-Bromanilino)acrolein which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C15H12Br2N2 (60670-67-9) → β-(m-Bromanilino)acrolein (51217-98-2) + m-Bromoaniline (591-19-5)

Guidance literature:

With water; sodium acetate; acetic acid; In ethanol; at 70 ℃; for 38h;

DOI:10.1248/cpb.28.2356

Reference yield:

m-Bromoaniline (591-19-5) + 3-ethoxyacrolein (19060-08-3) → β-(m-Bromanilino)acrolein (51217-98-2)

Guidance literature:

With sodium hydrogencarbonate; In methanol;

DOI:10.1248/cpb.21.2105

upstream raw materials:

m-Bromoaniline

3-ethoxyacrolein

C₁₅H₁₂Br₂N₂

Refernces

• 1、 Tamura,Yabe. "β Arylaminoacrolein derivatives. I. The investigation of Combes reaction and the syntheses of β arylaminoacrolein derivatives as the possible reactant". . p. 2105 - 2111. Retrieved 2007/10/05.