C₃₄H₃₁BF₂N₂O₃

Base Information

• Chemical Name: C₃₄H₃₁BF₂N₂O₃
• CAS No.: 1384575-77-2
• Molecular Formula: C₃₄H₃₁BF₂N₂O₃
• Molecular Weight: 564.44
• Mol file: 1384575-77-2.mol

Synonyms:C₃₄H₃₁BF₂N₂O₃

Chemical Property of C₃₄H₃₁BF₂N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₄H₃₁BF₂N₂O₃

There total 1 articles about C₃₄H₃₁BF₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2,4-dimethyl-1H-pyrrole (625-82-1) + C22H18O4 (1384516-74-8) → C34H31BF2N2O3 (1384575-77-2)

Guidance literature:

2,4-dimethyl-1H-pyrrole; C₂₂H₁₈O₄; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 11h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In toluene; for 0.5h;

DOI:10.1021/ja212125w

Reference yield:

C34H31BF2N2O3 (1384575-77-2) → C20H19BF2N2O3 (1384575-81-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; at 20 ℃; for 17h;

DOI:10.1021/ja212125w

Reference yield:

C34H31BF2N2O3 (1384575-77-2) → C34H27BF2N6O11 (1384575-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 17 h / 20 °C

2: potassium carbonate / acetone / 1 h / 20 - 80 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; dichloromethane; acetone;

DOI:10.1021/ja212125w

upstream raw materials:

2,4-dimethyl-1H-pyrrole

C₂₂H₁₈O₄

Downstream raw materials:

C₂₀H₁₉BF₂N₂O₃

C₃₄H₂₇BF₂N₆O₁₁

C₂₇H₂₃BF₂N₄O₇